Date of Award
Master of Arts
Dr. Donald Brown
Dr. Ralph K. Steinhaus
Dr. Dean W. Cooke
Masters Thesis-Open Access
This is a report of the synthesis and separation of transition metal complexes of hydrotris(1-pyrazolyl)- borate and hydrotris(3,5-dimethyl-l-pyrazolyl)borate. These complexes contain a central metal ion and two tridentate ligands, one hydrotris(1-pyrazolyl)borate and one hydrotris(3,5-dimethyl-l-pyrazolyl)borate. Mass spectrometry proved to be an extremely useful technique for identifying products. Many mass spectra are included and discussed extensively.
Complexes containing hydrobis(pyrazole)(3,5-dimethyl -1-pyrazolyl)borate and hydrobis(3,5-dimethyl-l-pyrazole) (pyrazolyl)borate also were synthesised and mass spectra obtained.
Alway, "The Synthesis and Characterization of Some Transition Metal Complexes Prom Mixtures of Poly Pyrazolyl Borates" (1984). Master's Theses. 1457.